Microstructure and Properties of PCrNi3Mo Steel Surface Layer after Two-Stage Vacuum Nitriding under Different Nitriding Time Conditions
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摘 要
采用二段式真空渗氮工艺对调质态PCrNi3Mo钢进行表面改性处理,在渗氮温度及氮势相同的条件下,对比研究了强渗阶段和扩散阶段时间均为6 h以及强渗阶段时间为4 h和扩散阶段时间为8 h条件下试验钢表层的组织、物相组成、硬度及耐磨性能。结果表明:渗氮后试验钢表层物相为ε-Fe2-3N相,2种渗氮时间下渗氮层的厚度分别为0.6,0.7 mm左右,表面硬度分别为660.3,581.3 HV,显著高于基体的360 HV;前者渗氮时间下渗氮层中化合物层致密性较差,微孔较多,渗氮层硬度过渡良好,在距表面距离大于0.3 mm时的硬度较高,渗氮层的摩擦因数和磨损量较低,磨损表面犁沟较浅,耐磨性能较好。
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Abstract
Two-stage vacuum nitriding process was used to modify the surface of quenched and tempered PCrNi3Mo steel. Under the condition of the same nitriding temperature and nitrogen potential, the microstructure, phase composition, hardness and wear resistance of the surface layer of the test steel were studied under the conditions of strong infiltration for 6 h and diffusion for 6 h, and compared with those by strong infiltration for 4 h and diffusion for 8 h. The results show that after nitriding, the phase of the test steel surface layer was ε-Fe2-3N phase. Under two nitriding time conditions, the thickness of nitrided layer was about 0.6, 0.7 mm, and the surface hardness was 660.3, 581.3 HV, respectively, higher than 360 HV of substrate. Under the former nitriding time condition, the compound layer in the nitriding layer had poor compactness and a great number of micropores; the hardness transition of the nitriding layer was good, and the hardness was relatively high at the distance from the surface of greater than 0.3 mm; the friction coefficient and wear amount of the nitrided layer were relatively low, and the furrow on the wear surface was shallow, indicating the wear resistance was relatively good.
中图分类号 TG156.8 DOI 10.11973/jxgccl202209002
所属栏目 试验研究
基金项目 辽宁省高等学校创新人才支持计划项目(LR 2019060)
收稿日期 2021/7/25
修改稿日期 2022/6/28
网络出版日期
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备注李振(1997-),男,辽宁锦州人,硕士研究生
引用该论文: LI Zhen,YANG Li,SHEN Tong,FENG Lingxiao. Microstructure and Properties of PCrNi3Mo Steel Surface Layer after Two-Stage Vacuum Nitriding under Different Nitriding Time Conditions[J]. Materials for mechancial engineering, 2022, 46(9): 11~15
李振,杨丽,沈统,冯凌宵. 不同渗氮时间下二段式真空渗氮后PCrNi3Mo钢表层的显微组织与性能[J]. 机械工程材料, 2022, 46(9): 11~15
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【3】许耀峰,单春来,刘朋科,等.火炮身管延寿方法研究综述[J].火炮发射与控制学报,2019,40(4):90-95. XU Y F,SHAN C L,LIU P K,et al.Review of the research on gun barrel life-span prolongation[J].Journal of Gun Launch & Control,2019,40(4):90-95.
【4】彭小敏,夏长清,吴安如,等.火炮身管烧蚀及其防护研究进展[J].四川兵工学报,2014,35(3):11-17. PENG X M,XIA C Q,WU A R,et al.Development of the ablation behavior and protection of gun barrel[J].Journal of Sichuan Ordnance,2014,35(3):11-17.
【5】WEIL H,BARRALLIER L,JÉGOU S,et al.Optimization of gaseous nitriding of carbon iron-based alloy based on fatigue resistance modelling[J].International Journal of Fatigue,2018,110:238-245.
【6】周上祺,侯琼,任勤.38CrMoAl钢离子渗氮微观结构的研究[J].金属热处理,2002,27(10):10-12. ZHOU S Q,HOU Q,REN Q.Microstructure of ion nitriding layer in 38CrMoAl steel[J].Heat Treatment of Metals,2002,27(10):10-12.
【7】戴海娜,许文花,肖桂勇,等.25Cr2MoVA钢气体渗氮工艺研究[J].材料热处理学报,2012,33(增刊2):113-116. DAI H N,XU W H,XIAO G Y,et al.Research on gas nitriding process of 25Cr2MoVA steel[J].Transactions of Materials and Heat Treatment,2012,33(S2):113-116.
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【15】刘建睿,严宏志,李算,等.离子渗氮工艺参数对4Cr5MoSiV钢表层组织与性能的影响[J].表面技术,2019,48(8):199-205. LIU J R,YAN H Z,LI S,et al.Effect of ion nitriding process parameters on surface properties of 4Cr5MoSiV steel[J].Surface Technology,2019,48(8):199-205.
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【17】李坤茂,颜志斌,刘静,等.温度对20CrMnTi钢渗氮层组织及耐磨性的影响[J].材料热处理学报,2018,39(11):80-86. LI K M,YAN Z B,LIU J,et al.Influence of temperature on microstructure and wear resistance of nitriding layer of 20CrMnTi steel[J].Transactions of Materials and Heat Treatment,2018,39(11):80-86.
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